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1094754-77-4

3-(4-Methyl-1H-indol-1-yl)propan-1-aMine synthesis

1synthesis methods
6089-09-4 Synthesis
4-PENTYNOIC ACID

6089-09-4
164 suppliers
$11.00/1g

3-(4-Methyl-1H-indol-1-yl)propan-1-aMine

1094754-77-4
5 suppliers
inquiry

5H-Pyrrolo[2',1':3,4][1,4]diazepino[1,2-a]indol-3(2H)-one, 1,6,7,13b-tetrahydro-12,13b-dimethyl-

1385027-59-7
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Yield:1385027-59-7 82%

Reaction Conditions:

Stage #1: 4-pentynoic acid;C12H16N2with 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride in water at 150; for 0.5 h;Microwave irradiation;
Stage #2: with trifluoroacetic acid in water at 150; for 0.5 h;Microwave irradiation;

References:

Feng, Enguang;Zhou, Yu;Zhao, Fei;Chen, Xianjie;Zhang, Lei;Jiang, Hualiang;Liu, Hong [Green Chemistry,2012,vol. 14,# 7,p. 1888 - 1895] Location in patent:supporting information; experimental part