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3,4-Pentadienal synthesis

2synthesis methods
-

Yield:4009-55-6 84%

Reaction Conditions:

with diisobutylaluminium hydride in dichloromethane at -90 - -80;

References:

Haydl, Alexander M.;Breit, Bernhard [Angewandte Chemie - International Edition,2015,vol. 54,# 51,p. 15530 - 15534][Angew. Chem.,2015,vol. 127,# 51,p. 15750 - 15754,5] Location in patent:supporting information