3,5-Dichloro-2,6-dihydroxybenzaldehyde synthesis
- Product Name:3,5-Dichloro-2,6-dihydroxybenzaldehyde
- CAS Number:1204298-54-3
- Molecular formula:C7H4Cl2O3
- Molecular Weight:207.01
100-97-0
0 suppliers
$14.00/250G
137-19-9
112 suppliers
$45.00/25g
1204298-54-3
7 suppliers
$75.00/1g
Yield:1204298-54-3 68%
Reaction Conditions:
Stage #1: hexamethylenetetramine;4,6-Dichlororesorcinol in trifluoroacetic acid at 70 - 100; for 76 h;Inert atmosphere;Duff Aldehyde Synthesis;
Stage #2: with hydrogenchloride;water in trifluoroacetic acid at 100; for 1 h;Duff Aldehyde Synthesis;
References:
Skonieczny, Kamil;Charalambidis, Georgios;Tasior, Mariusz;Krzeszewski, MacIej;Kalkan-Burat, Ayfer;Coutsolelos, Athanassios G.;Gryko, Daniel T. [Synthesis,2012,vol. 44,# 23,art. no. SS-2012-Z0640-OP,p. 3683 - 3687]