3-Acetyl-2(3H)-oxazolone synthesis
- Product Name:3-Acetyl-2(3H)-oxazolone
- CAS Number:60759-49-1
- Molecular formula:C5H5NO3
- Molecular Weight:127.1
60759-48-0
60759-49-1
The general procedure for the synthesis of 3-acetyloxazolidin-2-one from the compound (CAS:60759-48-0) is as follows: 6.80 g of 3-acetyl-5-chloro-oxazolidin-2-one was placed in a Kugelrohr distillation apparatus and distilled under reduced pressure conditions (50 mbar) and a temperature of 180°C. The product (3.80 g) was obtained from a Kugelrohr distillation apparatus. The final product 3-acetyloxazolidin-2-one (3.80 g) was obtained with a molecular weight of 127.1 g/mol (C5H5NO3).
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60759-49-1
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Yield:60759-49-1 172 g
Reaction Conditions:
Stage #1: 3-acetyl-1,3-oxazolidin-2-onewith chlorine in tetrachloromethane;UV-irradiation;
Stage #2: at 120 - 150;
References:
Scholz, Karl-Heinz;Heine, Hans-Georg;Hartmann, Willy [Organic Syntheses,1984,vol. 62,p. 149 - 149]
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60759-49-1
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60759-49-1
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$87.00/100mg