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874907-48-9

3-Bromo-1-fluoro-2-iodonaphthalene synthesis

3synthesis methods
13772-59-3 Synthesis
3-Bromo-1-fluoronaphthalene

13772-59-3
66 suppliers
$110.00/25mg

3-Bromo-1-fluoro-2-iodonaphthalene

874907-48-9
5 suppliers
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Yield:874907-48-9 80%

Reaction Conditions:

Stage #1: 3-bromo-1-fluoronaphthalenewith n-butyllithium;diisopropylamine in tetrahydrofuran;hexane at -75; for 2 h;
Stage #2: with iodine in tetrahydrofuran;hexane;

References:

Leroux, Frederic;Mangano, Giuseppe;Schlosser, Manfred [European Journal of Organic Chemistry,2005,# 23,p. 5049 - 5054]