3-bromo-2-cyanobenzyl bromide synthesis
1synthesis methods
- Product Name:3-bromo-2-cyanobenzyl bromide
- CAS Number:1243536-87-9
- Molecular formula:C8H5Br2N
- Molecular Weight:274.94
Yield:77532-81-1 46% ，1243536-87-9 44%
Reaction Conditions:
with N-Bromosuccinimide;dibenzoyl peroxide in tetrachloromethane;Inert atmosphere;Reflux;
References:
Noel, Timothy;Bert, Katrien;Van Der Eycken, Erik;Van Der Eycken, Johan [European Journal of Organic Chemistry,2010,# 21,p. 4056 - 4061] Location in patent:supporting information; experimental part