3-BROMO-4-HYDROXYBENZYLAMINE synthesis
- Product Name:3-BROMO-4-HYDROXYBENZYLAMINE
- CAS Number:63491-88-3
- Molecular formula:C7H8BrNO
- Molecular Weight:202.05
2973-78-6
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Yield:-
Reaction Conditions:
Stage #1: 3-bromo-4-hydroxybenzylaldehydewith Rink resin;trimethyl orthoformate at 25; for 2 h;
Stage #2: with lithium borohydride in tetrahydrofuran at 65; for 5 h;
Stage #3: with trifluoroacetic acid in dichloromethane at 25;
References:
Yraola, Francesc;García-Vicente, Silvia;Fernández-Recio, Juan;Albericio, Fernando;Zorzano, Antonio;Marti, Luc;Royo, Miriam [Journal of Medicinal Chemistry,2006,vol. 49,# 21,p. 6197 - 6208]
