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119405-32-2

3-BROMO-4-HYDROXYCINNAMIC ACID synthesis

4synthesis methods
2973-78-6 Synthesis
3-BROMO-4-HYDROXYBENZALDEHYDE

2973-78-6
224 suppliers
$14.00/5g

3-BROMO-4-HYDROXYCINNAMIC ACID

119405-32-2
11 suppliers
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Yield: 75%

Reaction Conditions:

with piperidine;pyridine at 80; for 5 h;

Steps:

4.2. Synthesis of 3-Br-pCA
201 mg (1 mmol) 3-bromo-4-hydroxybenzaldehyde (Sigma-Aldrich) and 229 mg (2.2 mmol) malonic acid (Sigma-Aldrich) was added to a 10 mL round-bottom flask containing a stir bar. 450 μL pyridine (J.T.Baker) and 18 μL piperidine (Sigma-Aldrich) was then added with stirring. The flask was submerged in a water bath held at 80 °C and refluxed for 5 h. The flask was then cooled to room temperature before dropwise addition of 9 mL 2M hydrochloric acid to produce a white precipitate. The solid was isolated with vacuum filtration, washed with additional 2M hydrochloric acid, and dried completely under vacuum, producing 181 mg of the desired 3-Br-pCA product (75 % yield). Any residual water in the product will prevent proper subsequent chromophore functionalization. LC-MS and 1H NMR data confirmed theidentity and purity (Fig. S1). The residual pyridinium salt detected in the 1H NMR spectrum does not interfere with any downstream reactions.

References:

Boxer, Steven G.;Lin, Chi-Yun;Romei, Matthew G. [Journal of Photochemistry and Photobiology A: Chemistry,2020,vol. 401]