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3-Bromo-5-methyl-2-thiophenecarboxaldehyde synthesis

2synthesis methods
13679-70-4 Synthesis
5-Methylthiophene-2-carboxaldehyde

13679-70-4
274 suppliers
$6.00/5g

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Yield:36155-82-5 65%

Reaction Conditions:

with N-Bromosuccinimide;palladium diacetate;silver trifluoroacetate;toluene-4-sulfonic acid;trifluoroacetic acid;4-Nitroanthranilic acid in 1,2-dichloro-ethane at 90; for 24 h;Sealed tube;

References:

Liu, Xi-Hai;Park, Hojoon;Hu, Jun-Hao;Hu, Yan;Zhang, Qun-Liang;Wang, Bao-Long;Sun, Bing;Yeung, Kap-Sun;Zhang, Fang-Lin;Yu, Jin-Quan [Journal of the American Chemical Society,2017,vol. 139,# 2,p. 888 - 896] Location in patent:supporting information

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