3-Bromo-6-(methoxymethoxy)-o-xylene synthesis
- Product Name:3-Bromo-6-(methoxymethoxy)-o-xylene
- CAS Number:1301147-34-1
- Molecular formula:C10H13BrO2
- Molecular Weight:245.11
22802-37-5
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1301147-34-1
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Yield:1301147-34-1 85%
Reaction Conditions:
Stage #1: 4-bromo-2,3-dimethylphenolwith sodium hydride in tetrahydrofuran;mineral oil at 0 - 23; for 0.833333 h;Inert atmosphere;
Stage #2: chloromethyl methyl ether in tetrahydrofuran;mineral oil at 23; for 2.16667 h;Inert atmosphere;
References:
Fujii, Seiko;Chang, Stephanie Y.;Burke, Martin D. [Angewandte Chemie - International Edition,2011,vol. 50,# 34,p. 7862 - 7864] Location in patent:supporting information; experimental part