3-bromo-6-(pyridin-3-yloxy)pyridine synthesis

1synthesis methods

Product Name:3-bromo-6-(pyridin-3-yloxy)pyridine
CAS Number:900493-23-4
Molecular formula:C10H7BrN2O
Molecular Weight:251.08

109-00-2
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$10.00/10g

624-28-2 Synthesis

624-28-2
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$5.00/5g

900493-23-4
18 suppliers
$157.00/1g

Yield:900493-23-4 66%

Reaction Conditions:

Stage #1: 3-HYDROXYPYRIDINEwith sodium hydride in N,N-dimethyl-formamide at 20; for 1 h;
Stage #2: 2,5-dibromopyridine in N,N-dimethyl-formamide; for 48 h;Heating;

References:

Voisin, Anne Sophie;Bouillon, Alexandre;Lancelot, Jean-Charles;Lesnard, Aurélien;Rault, Sylvain [Tetrahedron,2006,vol. 62,# 25,p. 6000 - 6005]

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