3-CHLORO-2-PYRROLIDIN-1-YL-PHENYLAMINE synthesis
- Product Name:3-CHLORO-2-PYRROLIDIN-1-YL-PHENYLAMINE
- CAS Number:58785-05-0
- Molecular formula:C10H13ClN2
- Molecular Weight:196.68
59504-30-2
7 suppliers
$23.30/250mg
58785-05-0
18 suppliers
$175.00/50mg
Yield:58785-05-0 95.1%
Reaction Conditions:
with Raney Ni in ethanol at 20;
Steps:
42.2
Step 2: A mixture of c (2.47 g, 1.09 mmol, 1.0 eq) and Raney-Ni (100 mg) in EtOH (80 mL) was was stirred at rt overnight. The reaction mixture was filtered. The filtrate was concentrated to afford d (2.04 g, 95.1 %). LCMS: 197.3 [M+H]+.
References:
WO2020/232375,2020,A1 Location in patent:Page/Page column 144
2106-49-2
188 suppliers
$5.00/5g
58785-05-0
18 suppliers
$175.00/50mg