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471-10-3

3-chloro-3,7-dimethylocta-1,6-diene synthesis

11synthesis methods
-

Yield:5389-87-7 69 %Spectr. ,39864-10-3 10 %Spectr. ,471-10-3 9 %Spectr.

Reaction Conditions:

Stage #1: Geraniolwith potassium hydride in 1,4-dioxane;Inert atmosphere;
Stage #2: with niobium pentachloride in 1,4-dioxane;Inert atmosphere;

References:

Ravikumar;Yao, Lihua;Fleming, Fraser F. [Journal of Organic Chemistry,2009,vol. 74,# 19,p. 7294 - 7299] Location in patent:supporting information; experimental part