3-CHLORO-4-METHYLBENZAMIDE synthesis
- Product Name:3-CHLORO-4-METHYLBENZAMIDE
- CAS Number:24377-95-5
- Molecular formula:C8H8ClNO
- Molecular Weight:169.61
21423-81-4
127 suppliers
$9.00/1g
24377-95-5
20 suppliers
$28.60/250mg
Yield:24377-95-5 100%
Reaction Conditions:
with Acetaldehyde oxime in methanol at 65; for 4 h;
Steps:
General procedure: A typical reaction was carried out in a 10 mL flask. Benzonitrile (2 mmol), CuII-4 ? (0.2 g), acetaldoxime (6 mmol) and MeOH (4 mL) were stirred at 65 °C for 4 h. The solid was filtered, washed with MeOH and the filtrate evaporated. The residue was subjected to GC-MS analysis and NMR spectroscopy. The filtered catalyst can be recycled after drying at about 150 °C for 1 h.
References:
Kiss, árpád;Hell, Zoltán [Tetrahedron Letters,2011,vol. 52,# 45,p. 6021 - 6023] Location in patent:experimental part
39652-32-9
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21423-81-4
127 suppliers
$9.00/1g
24377-95-5
20 suppliers
$28.60/250mg
21423-81-4
127 suppliers
$9.00/1g
24377-95-5
20 suppliers
$28.60/250mg
117738-77-9
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95-74-9
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$9.00/25g
24377-95-5
20 suppliers
$28.60/250mg