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153624-42-1

3-Isobutylphenylboronic acid synthesis

2synthesis methods
-

Yield:153624-42-1 82%

Reaction Conditions:

Stage #1: 1-bromo-3-isobutylbenzenewith n-butyllithium in tetrahydrofuran at -78; for 0.666667 h;
Stage #2: with Triisopropyl borate in tetrahydrofuran at -78 - 20;
Stage #3: with hydrogenchloride in tetrahydrofuran;

References:

Gan, Yonghong;Spencer, Thomas A. [Journal of Organic Chemistry,2006,vol. 71,# 16,p. 5870 - 5875]