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ChemicalBook CAS DataBase List 3-(METHOXYCARBONYL)-5-METHYLPHENYLBORONIC ACID

3-(METHOXYCARBONYL)-5-METHYLPHENYLBORONIC ACID synthesis

3synthesis methods
929626-17-5 Synthesis
3-METHOXYCARBONYL-5-METHYLPHENYLBORONIC ACID PINACOL ESTER

929626-17-5
41 suppliers
$80.00/500mg

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Yield:929626-18-6 466 mg

Reaction Conditions:

Stage #1: methyl 3-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoatewith sodium periodate;water in tetrahydrofuran at 23; for 8 h;Inert atmosphere;
Stage #2: with hydrogenchloride in tetrahydrofuran;water; for 1 h;Inert atmosphere;

References:

Furuya, Takeru;Ritter, Toblas [Organic Letters,2009,vol. 11,# 13,p. 2860 - 2863] Location in patent:supporting information; experimental part

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