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ChemicalBook CAS DataBase List 3-METHYL-2-BUTENE-1-AMINE HCL

3-METHYL-2-BUTENE-1-AMINE HCL synthesis

4synthesis methods
15936-45-5 Synthesis
N-(3-Methyl-2-butenyl)phthalimide

15936-45-5
13 suppliers
$90.00/100mg

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Yield: 78%

Reaction Conditions:

Stage #1:N-prenylphthalimide with hydrazine hydrate in ethanol;water for 1 h;Reflux;
Stage #2: with hydrogenchloride in ethanol;water for 1 h;Reflux;

References:

Coxon, Geoffrey D.;Furman, Brian L.;Harvey, Alan L.;McTavish, John;Mooney, Mark H.;Arastoo, Mahmoud;Kennedy, Alan R.;Tettey, Justice M.;Waigh, Roger D. [Journal of Medicinal Chemistry,2009,vol. 52,# 11,p. 3457 - 3463] Location in patent:supporting information; experimental part

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