3-METHYL-2-PHENYLVALERIC ACID synthesis
- Product Name:3-METHYL-2-PHENYLVALERIC ACID
- CAS Number:7782-37-8
- Molecular formula:C12H16O2
- Molecular Weight:192.25
Yield:7782-37-8 96%
Reaction Conditions:
Stage #1: phenylacetic acidwith n-butyllithium in tetrahydrofuran at 0; for 1.5 h;Inert atmosphere;
Stage #2: 2-butyl iodide in tetrahydrofuran; for 0.25 h;Inert atmosphere;
References:
Staudaher, Nicholas D.;Lovelace, Joseph;Johnson, Michael P.;Louie, Janis [Organic Syntheses,2017,vol. 94,p. 1 - 15]
5558-32-7
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