3-METHYLINDENE-2-CARBOXYLIC ACID synthesis
- Product Name:3-METHYLINDENE-2-CARBOXYLIC ACID
- CAS Number:34225-81-5
- Molecular formula:C11H10O2
- Molecular Weight:174.2
3666-82-8
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34225-81-5
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Yield:34225-81-5 85%
Reaction Conditions:
Stage #1: 2-benzyl-3-oxo-butyric acid methyl esterwith trifluorormethanesulfonic acid in dichloromethane at 0 - 25;
Stage #2: with trifluoroacetic acid in dichloromethane at 25; for 8 h;
References:
Kurouchi, Hiroaki;Sugimoto, Hiromichi;Otani, Yuko;Ohwada, Tomohiko [Journal of the American Chemical Society,2010,vol. 132,# 2,p. 807 - 815] Location in patent:supporting information; experimental part
2382-58-3
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34225-81-5
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7316-64-5
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34225-81-5
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