3-NITROPHENYLSULFUR PENTAFLUORIDE synthesis
- Product Name:3-NITROPHENYLSULFUR PENTAFLUORIDE
- CAS Number:2613-26-5
- Molecular formula:C6H4F5NO2S
- Molecular Weight:249.16
2557-81-5
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2613-26-5
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Yield: 100%
Reaction Conditions:
with nitronium tetrafluoborate;trifluorormethanesulfonic acid in dichloromethane at 20; for 24 h;Reagent/catalyst;Solvent;Temperature;Time;
Steps:
5
PhSF5 15 reacts with NO2+BF4/TfOH in CH2Cl2 at room temperature to give 1-nitro-3-(pentafluorosulfanyl)benzene 16 in near quantitative yield, as seen in Table 6.
References:
University of North Florida;Laali, Kenneth K. US9238660, 2016, B1 Location in patent:Page/Page column 10; 11
537-91-7
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2613-26-5
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$15.00/1g
2557-81-5
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$25.00/250mg
142653-59-6
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349-78-0
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2613-26-5
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2613-26-5
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