3-propan-2-ylcyclohex-2-en-1-one synthesis
- Product Name:3-propan-2-ylcyclohex-2-en-1-one
- CAS Number:6328-22-9
- Molecular formula:C9H14O
- Molecular Weight:138.21
![Cyclohexene, 1-[(triethylsilyl)oxy]-](/CAS/20210305/GIF/4342-22-7.gif)
4342-22-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: o-iodoxybenzoic acid (IBX); 4-methoxypyridine N-oxide / dimethylsulfoxide; CH2Cl2 / 8 h / 25 °C
2.1: CuBr*SMe2 / tetrahydrofuran / 0.5 h / -78 °C
2.2: N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran / 0.5 h / -78 - 25 °C
3.1: o-iodoxybenzoic acid / dimethylsulfoxide / 20 °C
References:
Nicolaou;Gray, David L. F.;Montagnon, Tamsyn;Harrison, Scott T. [Angewandte Chemie - International Edition,2002,vol. 41,# 6,p. 996 - 1000]
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1000210-73-0
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6328-22-9
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23074-59-1
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$65.00/50mg
1068-55-9
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$20.00/25ml
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16566-96-4
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