3-Pyridinol, 6-(4-morpholinyl)- synthesis
- Product Name:3-Pyridinol, 6-(4-morpholinyl)-
- CAS Number:755034-16-3
- Molecular formula:C9H12N2O2
- Molecular Weight:180.2
41288-96-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 25 h / 40 °C
2: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl / toluene / 24 h / 85 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 17 h / 37503.8 Torr
References:
CN109251166,2019,A
84611-43-8
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