
3-(TRIFLUOROMETHYL)BENZOPHENONE synthesis
- Product Name:3-(TRIFLUOROMETHYL)BENZOPHENONE
- CAS Number:728-81-4
- Molecular formula:C14H9F3O
- Molecular Weight:250.22

728-80-3
96 suppliers
$10.00/1g

728-81-4
73 suppliers
$15.00/5g
Yield: 99%
Reaction Conditions:
with N-Bromosuccinimide;potassium acetate in dichloromethane;water at 20; for 10 h;Green chemistry;
Steps:
General Procedure for the Oxidative Reaction
General procedure: A solution of diphenylmethanol (1 mmol), NBS (1.3equiv.), KOAc (1.5 equiv.) H2O (1.5 mL), and CH2Cl2 (0.5mL) was magnetically stirred in 25 mL flask at room temperaturefor 10 h. The reaction mixture was added into water(10 mL), and extracted with EtOAc (3 × 10 mL). The combinedEtOAc extracts were dried over anhydrous MgSO4,filtrated, and then the solvent was removed under reducedpressure. The residue was purified by the flash columnchromatography on silica gel with PE or PE/EtOAc as theeluent to obtain the desired products. The oxidation productswere identified by GC-MS and 1H NMR.
References:
Wu, Jianglong;Liu, Yan;Liu, Ping;Gu, Chengzhi [Letters in Organic Chemistry,2017,vol. 14,# 4,p. 254 - 260]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
0 suppliers
inquiry

728-81-4
73 suppliers
$15.00/5g

2251-65-2
222 suppliers
$10.00/1g

100-58-3
196 suppliers
$18.00/10ml

728-81-4
73 suppliers
$15.00/5g

340136-34-7
9 suppliers
$424.00/100g

100-58-3
196 suppliers
$18.00/10ml

728-81-4
73 suppliers
$15.00/5g