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ChemicalBook CAS DataBase List 3-Boric acid triphenylamine pinesol ester
915088-14-1

3-Boric acid triphenylamine pinesol ester synthesis

4synthesis methods
61676-62-8 Synthesis
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

61676-62-8
318 suppliers
$11.19/5G

78600-33-6 Synthesis
3-BROMO-N N-DIPHENYLANILINE  97

78600-33-6
112 suppliers
$24.00/1g

3-Boric acid triphenylamine pinesol ester

915088-14-1
21 suppliers
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Yield:915088-14-1 80%

Reaction Conditions:

Stage #1: N-3-bromophenyl-N,N-diphenylaminewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;Inert atmosphere;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran;hexane at -78 - 20;Inert atmosphere;

References:

Zhu, Minrong;Li, Yanhu;Hu, Sujun;Li, Chen'Ge;Yang, Chuluo;Wu, Hongbin;Qin, Jingui;Cao, Yong [Chemical Communications,2012,vol. 48,# 21,p. 2695 - 2697] Location in patent:supporting information; experimental part