ChemicalBook CAS DataBase List Benzoic acid, 5-bromo-2-[[(1,1-dimethylethoxy)carbonyl]amino]- (9CI)

Benzoic acid, 5-bromo-2-[[(1,1-dimethylethoxy)carbonyl]amino]- (9CI) synthesis

1synthesis methods

Product Name:Benzoic acid, 5-bromo-2-[[(1,1-dimethylethoxy)carbonyl]amino]- (9CI)
CAS Number:306937-20-2
Molecular formula:C12H14BrNO4
Molecular Weight:316.15

118-92-3
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$23.00/250g

Benzoic acid, 5-bromo-2-[[(1,1-dimethylethoxy)carbonyl]amino]- (9CI)

306937-20-2
69 suppliers
$27.00/250mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 95 percent / [bmim]Br₃ / CH₂Cl₂ / 0.67 h / 20 °C
2: 60 percent / Na₂CO₃ / CH₂Cl₂ / 25 h / 20 - 40 °C

References:

Egger, Michael;Li, Xuqin;Mueller, Christine;Bernhardt, Guenther;Buschauer, Armin;Koenig, Burkhard [European Journal of Organic Chemistry,2007,# 16,p. 2643 - 2649]

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