2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester synthesis
- Product Name:2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester
- CAS Number:34874-90-3
- Molecular formula:C10H10O5
- Molecular Weight:210.18
Yield:34874-90-3 87%
Reaction Conditions:
Stage #1: methyl orsellinatewith titanium tetrachloride in dichloromethane at 0; for 0.166667 h;Inert atmosphere;
Stage #2: Dichloromethyl methyl ether in dichloromethane at 0 - 20; for 1 h;Inert atmosphere;
References:
Dong, Chunmao;Huo, Luqiong;Liu, Hongxin;Lu, Xiuxiang;Qiu, Shengxiang;Tan, Haibo;Wang, Miaomiao;Yang, Bao;Yuan, Yunfei;Zhang, Wenge [Organic Letters,2020] Location in patent:supporting information
4885-02-3
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