(2R,5S)-2-(1-Mercapto-1-methylethyl)-5-methylcyclohexanone synthesis
1synthesis methods
- Product Name:(2R,5S)-2-(1-Mercapto-1-methylethyl)-5-methylcyclohexanone
- CAS Number:35117-86-3
- Molecular formula:C10H18OS
- Molecular Weight:186.31
Yield:20 % de
Reaction Conditions:
with aluminum (III) chloride;hydrogen sulfide in dichloromethane at 60; for 3 h;Autoclave;Overall yield = 65 %; Overall yield = 2.8 g;
References:
Emura, Makoto;Matsuda, Hiroyuki [Chemistry and Biodiversity,2014,vol. 11,# 11,p. 1688 - 1699]