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ChemicalBook CAS DataBase List (2R,5S)-2-(1-Mercapto-1-methylethyl)-5-methylcyclohexanone
35117-86-3

(2R,5S)-2-(1-Mercapto-1-methylethyl)-5-methylcyclohexanone synthesis

1synthesis methods
-

Yield:20 % de

Reaction Conditions:

with aluminum (III) chloride;hydrogen sulfide in dichloromethane at 60; for 3 h;Autoclave;Overall yield = 65 %; Overall yield = 2.8 g;

References:

Emura, Makoto;Matsuda, Hiroyuki [Chemistry and Biodiversity,2014,vol. 11,# 11,p. 1688 - 1699]