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35813-68-4

4,5-DIHYDRO-2-(ETHOXYCARBONYL)NAPTHO(1,2-B)THIOPENE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 87.5 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl4 / 0.75 h / Heating
2: 87.2 percent / LiAlH4 / tetrahydrofuran; diethyl ether / 3.5 h / Heating

References:

Carpino, Louis A.;Abdel-Maksoud, Adel Ali;Ionescu, Dumitru;Mansour;Zewail, Mohamed A. [Journal of Organic Chemistry,2007,vol. 72,# 5,p. 1729 - 1736]

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