ChemicalBook CAS DataBase List 4-(2-methoxyphenyl)-3-thiophen-2-yl-1H-1,2,4-triazole-5-thione

4-(2-methoxyphenyl)-3-thiophen-2-yl-1H-1,2,4-triazole-5-thione synthesis

1synthesis methods

Product Name:4-(2-methoxyphenyl)-3-thiophen-2-yl-1H-1,2,4-triazole-5-thione
CAS Number:380574-16-3
Molecular formula:C13H11N3OS2
Molecular Weight:289.38

N-(2-methoxyphenyl)-2-(thiophen-2-ylcarbonyl)hydrazinecarbothioamide

516458-34-7
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4-(2-methoxyphenyl)-3-thiophen-2-yl-1H-1,2,4-triazole-5-thione

380574-16-3
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Yield:380574-16-3 87%

Reaction Conditions:

with sodium hydroxide in water; for 2 h;Reflux;

References:

Siwek, Agata;Wujec, Monika;Dobosz, Maria;Jagiello-Wojtowicz, Ewa;Kleinrok, Agnieszka;Chodkowska, Anna;Paneth, Piotr [Phosphorus, Sulfur and Silicon and the Related Elements,2008,vol. 183,# 11,p. 2669 - 2677] Location in patent:experimental part

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