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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
38145-93-6

(R)-1-[(4R,4'R)-2,2,2',2'-Tetramethyl-4α,4'β-bi[1,3-dioxolane]-5β-yl]ethane-1,2-diol synthesis

6synthesis methods
1,2:3,4:5,6-TRI-O-ISOPROPYLIDENE-D-MANNITOL

3969-59-3
42 suppliers
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(R)-1-[(4R,4'R)-2,2,2',2'-Tetramethyl-4α,4'β-bi[1,3-dioxolane]-5β-yl]ethane-1,2-diol

38145-93-6
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Yield:38145-93-6 92%

Reaction Conditions:

with sulfuric acid;silica gel in methanol at 20;chemoselective reaction;

References:

Vidyasagar, Adiyala;Pathigoolla, Atchutarao;Sureshan, Kana M. [Organic and Biomolecular Chemistry,2013,vol. 11,# 33,p. 5443 - 5453]

69-65-8 Synthesis
D-Mannitol

69-65-8
730 suppliers
$5.00/25g

(R)-1-[(4R,4'R)-2,2,2',2'-Tetramethyl-4α,4'β-bi[1,3-dioxolane]-5β-yl]ethane-1,2-diol

38145-93-6
1 suppliers
inquiry

References
69-65-8 Synthesis
D-Mannitol

69-65-8
730 suppliers
$5.00/25g

116-11-0 Synthesis
2-Methoxypropene

116-11-0
279 suppliers
$10.00/5g

D-Mannitol, 1,2:4,6-bis-O-(1-methylethylidene)-

92218-94-5
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(R)-1-[(4R,4'R)-2,2,2',2'-Tetramethyl-4α,4'β-bi[1,3-dioxolane]-5β-yl]ethane-1,2-diol

38145-93-6
1 suppliers
inquiry

1707-77-3 Synthesis
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol

1707-77-3
370 suppliers
$5.00/5g

1,2:3,4:5,6-TRI-O-ISOPROPYLIDENE-D-MANNITOL

3969-59-3
42 suppliers
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References
1,2:3,4:5,6-TRI-O-ISOPROPYLIDENE-D-MANNITOL

3969-59-3
42 suppliers
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3,4-O-ISOPROPYLIDENE-D-MANNITOL

3969-84-4
100 suppliers
$33.50/1g

(R)-1-[(4R,4'R)-2,2,2',2'-Tetramethyl-4α,4'β-bi[1,3-dioxolane]-5β-yl]ethane-1,2-diol

38145-93-6
1 suppliers
inquiry

References
69-65-8 Synthesis
D-Mannitol

69-65-8
730 suppliers
$5.00/25g

2,2-Dimethoxypropane

77-76-9
400 suppliers
$9.00/5ml

1,2-O-ISOPROPYLIDENE-D-MANNITOL

4306-35-8
27 suppliers
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(R)-1-[(4R,4'R)-2,2,2',2'-Tetramethyl-4α,4'β-bi[1,3-dioxolane]-5β-yl]ethane-1,2-diol

38145-93-6
1 suppliers
inquiry

1707-77-3 Synthesis
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol

1707-77-3
370 suppliers
$5.00/5g

1,2:3,4:5,6-TRI-O-ISOPROPYLIDENE-D-MANNITOL

3969-59-3
42 suppliers
inquiry

References