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ChemicalBook CAS DataBase List 4-[2-(4-AMINOPHENYL)ETHYL]PHENOL
33384-05-3

4-[2-(4-AMINOPHENYL)ETHYL]PHENOL synthesis

5synthesis methods
-

Yield:33384-05-3 100 %Chromat.

Reaction Conditions:

Stage #1: p-benzyloxystyrene;para-nitrophenyl bromidewith 5% Pd(II)/C(eggshell);sodium acetate in 1-methyl-pyrrolidin-2-one at 140; for 24 h;Heck reaction;
Stage #2: with 5% Pd(II)/C(eggshell);hydrogen in 1-methyl-pyrrolidin-2-one at 20; under 750.075 Torr; for 24 h;

References:

Cusati, Giuseppe;Wedig, Anja;Djakovitch, Laurent [Letters in Organic Chemistry,2009,vol. 6,# 1,p. 77 - 81] Location in patent:scheme or table