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4-(2-NAPHTHYL)-1-BUTENE synthesis

11synthesis methods
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Yield:2489-89-6 85%

Reaction Conditions:

Stage #1: β-naphthaldehyde;allylsamarium bromide in tetrahydrofuran at 20; for 0.5 h;Inert atmosphere;
Stage #2: with phosphonic acid diethyl ester in tetrahydrofuran;Inert atmosphere;

References:

Li, Ying;Hu, Yuan-Yuan;Zhang, Song-Lin [Chemical Communications,2013,vol. 49,# 90,p. 10635 - 10637] Location in patent:supporting information

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