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4-(4-AZIDOPHENYL)BUTYRIC ACID synthesis

2synthesis methods
-

Yield:103489-33-4 71%

Reaction Conditions:

Stage #1: 4-(4-aminophenyl)butyric Acidwith sulfuric acid;sodium nitrite at 0; for 0.75 h;Diazotization;
Stage #2: with sodium azide at 0; for 0.666667 h;Substitution;

References:

Halmos, Therese;Turek, Joseph W.;Le Breton, Guy C.;Antonakis, Kostas [Bioorganic and Medicinal Chemistry Letters,1999,vol. 9,# 20,p. 2963 - 2968]