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ChemicalBook CAS DataBase List 4,4-Dioctyl-4H-silolo[3,2-b:4,5-b']dithiophene
1160106-12-6

4,4-Dioctyl-4H-silolo[3,2-b:4,5-b']dithiophene synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Schlenk technique
1.2: 3 h / 20 °C / Inert atmosphere; Schlenk technique
2.1: trifluoroacetic acid / chloroform / 3 h / 20 °C

References:

Caselli, Monica;Vanossi, Davide;Buffagni, Mirko;Imperato, Manuel;Pigani, Laura;Mucci, Adele;Parenti, Francesca [ChemPlusChem,2019,vol. 84,# 9,p. 1314 - 1323]