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ChemicalBook CAS DataBase List 4,5‐ b']difuran

4,5‐ b']difuran synthesis

2synthesis methods
1391764-82-1 Synthesis
IN1532, 4,8-Bis(5-(2-ethylhexyl)thiophen-2-yl)benzo[1,2-b:4,5-b']difuran

1391764-82-1
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4,5‐
b']difuran

1391764-83-2
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Yield:1391764-83-2 77%

Reaction Conditions:

Stage #1: 4,8-bis(5-(2-ethylhexyl)thiophen-2-yl)benzo[1,2-b;4,5-b′]difuranwith n-butyllithium in tetrahydrofuran at 0 - 20; for 2 h;
Stage #2: trimethyltin(IV)chloride in tetrahydrofuran;hexane at 20; for 1 h;

References:

Huo, Lijun;Ye, Long;Wu, Yue;Li, Zhaojun;Guo, Xia;Zhang, Maojie;Zhang, Shaoqing;Hou, Jianhui [Macromolecules,2012,vol. 45,# 17,p. 6923 - 6929]

4891-44-5 Synthesis
2-(2-Ethylhexyl)thiophene

4891-44-5
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$21.00/250mg

267220-47-3 Synthesis
4,5-b']difuran-4,8-dione

267220-47-3
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4,5‐
b']difuran

1391764-83-2
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