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4161-32-4

4,8-dioxaundecane-1,11-diol synthesis

10synthesis methods
-

Yield:4161-32-4 79%

Reaction Conditions:

Stage #1: C13H24O6with lithium aluminium tetrahydride
Stage #2: with water

Steps:



Compound 97 (4,8-dioxaundecane-l,ll-diol) was synthesized in three steps using established methods[33] as shown in Figure 12 - Scheme 12: (a) acrylonitrile, 2%w/v sodium hydroxide; (b) cone, sulfuric acid, 95% ethanol; (c) lithium aluminium hydride.

References:

WO2009/152392,2009,A2 Location in patent:Page/Page column 25