4-ACETAMIDOBENZYL ALCOHOL synthesis
- Product Name:4-ACETAMIDOBENZYL ALCOHOL
- CAS Number:16375-88-5
- Molecular formula:C9H11NO2
- Molecular Weight:165.19
623-04-1
363 suppliers
$6.00/1g
108-24-7
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$14.00/250ML
16375-88-5
108 suppliers
$22.00/1g
Yield: 98%
Reaction Conditions:
with Co3O4 nanoparticles at 20; for 0.2 h;Green chemistry;chemoselective reaction;
Steps:
General procedure for acetylation of amines
General procedure: In a round-bottomed flask (25 mL) equipped with a magnetic stirrer, a mixture of aniline (0.093 g, 1 mmol) and Co3O4 (0.006 g) was prepared. Acetic anhydride (0.102, 1 mmol) was then added to the reaction mixture and stirring was continued at room temperature for 3 min. The progress of the reaction was followed by TLC. After the reaction completion, the products was extracted with EtOAc and filtered to remove Co3O4. The organic solvent was then washed with H2O (2 x 10 mL) and saturated NaHCO3 solution and then dried over anhydrous Na2SO4. The solvent was removed under vacuum to afford the pure product.
References:
Marjani, Ahmad Poursattar;Hosseini, Seyed Ali;Shokri, Zahra;Maleki, Nasim [Research on Chemical Intermediates,2017,vol. 43,# 1,p. 413 - 422]
122-85-0
229 suppliers
$10.00/1g
16375-88-5
108 suppliers
$22.00/1g
623-04-1
363 suppliers
$6.00/1g
10387-40-3
364 suppliers
$10.00/1g
16375-88-5
108 suppliers
$22.00/1g
