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ChemicalBook CAS DataBase List 4-AMINOBENZOIC-2, 3, 5, 6-D4 ACID

4-AMINOBENZOIC-2, 3, 5, 6-D4 ACID synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: nitric acid; sulfuric acid / 4.67 h / 5 - 25 °C
2: magnesium sulfate heptahydrate; potassium permanganate / water / 2.5 h / 85 °C
3: ammonium formate; palladium 10% on activated carbon / methanol; water / 0.33 h / 90 - 100 °C / Microwave irradiation

References:

Havaldar, Freddy H.;Dabholkar, Bhushan Vasant;Mule, Ganesh Baban;Kulkarni, Suhas [Journal of labelled compounds and radiopharmaceuticals,2015,vol. 58,# 4,p. 163 - 165]

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