ChemicalBook CAS DataBase List 4-AMINOBUTYRIC-2,2-D2 ACID

4-AMINOBUTYRIC-2,2-D2 ACID synthesis

1synthesis methods

Product Name:4-AMINOBUTYRIC-2,2-D2 ACID
CAS Number:67910-98-9
Molecular formula:C4H7D2NO2
Molecular Weight:105.13

Propanoic-2,2,3,3-d4 acid, 3-cyano-, ethyl ester

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Yield:67910-98-9 48%

Reaction Conditions:

Stage #1: ethyl [2,2,3,3-⁽²⁾H₄]-3-cyanopropanoatewith water;sodium hydroxide for 1.5 h;Reflux;
Stage #2: with sodium borodeuteride;cobalt(II) chloride hexahydrate

References:

Cook, Matthew C.;Witherell, Ross D.;White, Robert L. [Letters in drug design and discovery,2010,vol. 7,# 1,p. 9 - 13] Location in patent:experimental part

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