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70076-04-9

(4-BroMo-3-nitro-phenyl)-diMethyl-aMine synthesis

4synthesis methods
-

Yield:70076-04-9 94%

Reaction Conditions:

Stage #1: 4-bromo-N,N-dimethylanilinewith tert-butyl methyl ether;nitric acid in tetrahydrofuran at 0;
Stage #2: with sulfuric acid in dichloromethane at 0; for 1 h;Further stages.;

References:

Zhang, Pingsheng;Cedilote, Miall;Cleary, Thomas P.;Pierce, Michael E. [Tetrahedron Letters,2007,vol. 48,# 49,p. 8659 - 8664]