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ChemicalBook CAS DataBase List 4-BROMO-7-METHYLTRYPTOPHOL

4-BROMO-7-METHYLTRYPTOPHOL synthesis

2synthesis methods
-

Yield:214915-69-2 25%

Reaction Conditions:

Stage #1: 2,3-dihydro-2H-furan;(5-bromo-2-methylphenyl)hydrazine in tetrahydrofuran;water at 0 - 20; for 14 h;
Stage #2: zinc(II) chloride in ethylene glycol at 170; for 4 h;

References:

WO2003/99275,2003,A1 Location in patent:Page 53

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