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ChemicalBook CAS DataBase List 4-Bromobenzo[a]anthracene

4-Bromobenzo[a]anthracene synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 97 percent / bromine / acetic acid / 4 h / Heating
2: 1.) hydroiodic acid, hypophosphorous acid, 2.) chloranil / 1.) acetic acid, reflux, 18 h, 2.) benzene, reflux, overnight

References:

Cho, Bongsup P.;Harvey, Ronald G. [Journal of Organic Chemistry,1987,vol. 52,# 26,p. 5668 - 5678]