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1609259-31-5

4-chloro-7-methoxy-1H-pyrazolo[4,3-c]pyridine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: dichloromethane / 18 h / 20 °C
2: nitric acid / sulfuric acid / 1 h / 0 - 90 °C
3: iron / acetic acid / 1 h / 100 °C
4: sodium nitrite / acetic acid; water / 1 h / 75 °C

References:

US2014/128374,2014,A1