4-DI-N-PROPYLAMINO-PIPERIDINE synthesis
- Product Name:4-DI-N-PROPYLAMINO-PIPERIDINE
- CAS Number:675136-96-6
- Molecular formula:C11H24N2
- Molecular Weight:184.32
1259401-76-7
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675136-96-6
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Yield:675136-96-6 80%
Reaction Conditions:
with palladium 10% on activated carbon;water in ethanol; under 15001.5 Torr; for 4 h;Reflux;Autoclave;
Steps:
1.G Step G: Preparation of N- (piperidin-4-yl) dipropylamine
To the autoclave, 0.34 mol of the compound of step F was added,Water 60% 10% Pd / C 10 g,Ethanol 1000ml,Pressurized to 2Mpa,Reflux reaction for 4 hours.Filtered and concentrated to give 50 g of product as a yellow oil in 80% yield.
References:
CN103130709,2017,B Location in patent:Paragraph 0157; 0158
3612-20-2
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675136-96-6
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$44.00/500mg
160358-05-4
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675136-96-6
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