ChemicalBook CAS DataBase List 4-diphenyl-1-naphthalene boronic acid

4-diphenyl-1-naphthalene boronic acid synthesis

3synthesis methods

Product Name:4-diphenyl-1-naphthalene boronic acid
CAS Number:881811-83-2
Molecular formula:C22H17BO2
Molecular Weight:324.18

881811-70-7
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881811-83-2
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: aq. H₂SO₄ / 8 h / 50 °C
1.2: aq. NaNO₂ / 0.5 h / 0 °C
1.3: 79 percent / aq. KI / 4 h / Heating
2.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C
2.2: hexane; tetrahydrofuran / 20 °C
3.1: 147 mg / aq. HCl / hexane; tetrahydrofuran

References:

Ooi, Takashi;Uematsu, Yukitaka;Maruoka, Keiji [Journal of the American Chemical Society,2006,vol. 128,# 8,p. 2548 - 2549]

3-(Dimethylamino)-1-(3-methoxyphenyl)-2-methyl-1-propanone

197145-37-2
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$175.96/250mg

881811-83-2
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References

809274-71-3
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881811-83-2
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References