4-ethoxy-N-methoxy-N-methylbenzamide synthesis
- Product Name:4-ethoxy-N-methoxy-N-methylbenzamide
- CAS Number:1221341-06-5
- Molecular formula:C11H15NO3
- Molecular Weight:209.24
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Yield:-
Reaction Conditions:
Stage #1: 4-(ethoxy)benzoic acidwith oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane at 20; for 3 h;Inert atmosphere;
Stage #2: O,N-dimethyl-hydroxylamine hydrochloridewith triethylamine in dichloromethane at 0;Inert atmosphere;
References:
Komatsuda, Masaaki;Kondo, Hiroki;Ohki, Hugo;Suto, Ayane;Yamaguchi, Junichiro [Organic Letters,2022,vol. 24,# 17,p. 3270 - 3274] Location in patent:supporting information