4'-FLUORO-3-(4-FLUOROPHENYL)PROPIOPHENONE synthesis
- Product Name:4'-FLUORO-3-(4-FLUOROPHENYL)PROPIOPHENONE
- CAS Number:104147-29-7
- Molecular formula:C15H12F2O
- Molecular Weight:246.25
352-34-1
368 suppliers
$7.00/5g
107-18-6
2 suppliers
$24.60/100ml
104147-29-7
9 suppliers
$467.00/1g
Yield: 42%
Reaction Conditions:
Stage #1:4-fluoro-1-iodobenzene;allyl alcohol with palladium diacetate;potassium carbonate in N,N-dimethyl-formamide at 110; for 0.0833333 h;Inert atmosphere;
Stage #2: with pyrrolidine in N,N-dimethyl-formamide at 110; for 24 h;Inert atmosphere;regioselective reaction;
References:
Zhu, Zhi-Qiang;He, Jian-Shi;Wang, Hai-Jun;Huang, Zhi-Zhen [Journal of Organic Chemistry,2015,vol. 80,# 18,p. 9354 - 9359]
462-06-6
412 suppliers
$10.00/5g
772-70-3
8 suppliers
$90.00/100mg
104147-29-7
9 suppliers
$467.00/1g