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4’-(Hydroxymethyl)-3’-vinylacetophenone synthesis

3synthesis methods
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Yield:1418144-63-4 10.7 g

Reaction Conditions:

with bis-triphenylphosphine-palladium(II) chloride;sodium carbonate in tetrahydrofuran;water at 80; for 5 h;

References:

Pan, Shifeng;Gray, Nathanael S.;Gao, Wenqi;Mi, Yuan;Fan, Yi;Wang, Xing;Tuntland, Tove;Che, Jianwei;Lefebvre, Sophie;Chen, Yu;Chu, Alan;Hinterding, Klaus;Gardin, Anne;End, Peter;Heining, Peter;Bruns, Christian;Cooke, Nigel G.;Nuesslein-Hildesheim, Barbara [ACS Medicinal Chemistry Letters,2013,vol. 4,# 3,p. 333 - 337] Location in patent:supporting information