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4-Iodo-1-methyl-1H-indazol-3-ylamine synthesis

1synthesis methods
-

Yield:796967-84-5 87%

Reaction Conditions:

in butan-1-ol at 100 - 110; for 3 h;

References:

Dai, Yujia;Hartandi, Kresna;Ji, Zhiqin;Ahmed, Asma A.;Albert, Daniel H.;Bauch, Joy L.;Bouska, Jennifer J.;Bousquet, Peter F.;Cunha, George A.;Glaser, Keith B.;Harris, Christopher M.;Hickman, Dean;Guo, Jun;Li, Junling;Marcotte, Patrick A.;Marsh, Kennan C.;Moskey, Maria D.;Martin, Ruth L.;Olson, Amanda M.;Osterling, Donald J.;Pease, Lori J.;Soni, Niru B.;Stewart, Kent D.;Stoll, Vincent S.;Tapang, Paul;Reuter, David R.;Davidsen, Steven K.;Michaelides, Michael R. [Journal of Medicinal Chemistry,2007,vol. 50,# 7,p. 1584 - 1597]