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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4-Iodo-1-methyl-3-nitro-1H-pyrazole synthesis

1synthesis methods
1H-Pyrazole,1-methyl-3-nitro-(9CI)

54210-32-1
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4-Iodo-1-methyl-3-nitro-1H-pyrazole

75092-34-1
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Yield:75092-34-1 79%

Reaction Conditions:

with sulfuric acid;iodine;iodic acid in tetrachloromethane;acetic acid at 80; for 1.5 h;

References:

Vasilevskii, S. F.;Shvartsberg, M. S. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1980,vol. 29,# 5,p. 778 - 784][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1980,# 5,p. 1071 - 1077]